2Y9Y
Chromatin Remodeling Factor ISW1a(del_ATPase)
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06SA |
| Synchrotron site | SLS |
| Beamline | X06SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2008-06-11 |
| Detector | DECTRIS PILATUS 6M |
| Spacegroup name | H 3 2 |
| Unit cell lengths | 206.971, 206.971, 215.308 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 29.874 - 3.250 |
| R-factor | 0.2838 |
| Rwork | 0.283 |
| R-free | 0.29650 |
| Structure solution method | MIRAS |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.002 |
| RMSD bond angle | 0.467 |
| Data reduction software | XDS |
| Data scaling software | SCALA |
| Phasing software | SHARP |
| Refinement software | PHENIX |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 30.000 | 3.360 |
| High resolution limit [Å] | 3.250 | 3.250 |
| Rmerge | 0.070 | 0.310 |
| Number of reflections | 28004 | |
| <I/σ(I)> | 3.6 | 2.2 |
| Completeness [%] | 100.0 | 100 |
| Redundancy | 10.9 | 11.2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 6.5 | 100MM BISTRIS, PH 7.0, 1.6M NA-CITRATE, 10% GLYCEROL, 0.1M NA PHOSPHATE. |
