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2Y9R

Crystal structure of the M10 domain of Titin

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsDIAMOND BEAMLINE I04
Synchrotron siteDiamond
BeamlineI04
Temperature [K]100
Detector technologyCCD
Collection date2009-04-04
DetectorADSC CCD
Spacegroup nameP 42
Unit cell lengths43.450, 43.450, 56.380
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution34.420 - 1.900
R-factor0.19592
Rwork0.194
R-free0.24108
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)2wp3
RMSD bond length0.015
RMSD bond angle1.543
Data reduction softwareMOSFLM
Data scaling softwareSCALA
Phasing softwareMOLREP
Refinement softwareREFMAC (5.6.0101)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]34.4202.000
High resolution limit [Å]1.9001.900
Rmerge0.0900.550
Number of reflections8350
<I/σ(I)>10.83
Completeness [%]99.9100
Redundancy55.1
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
16.535% PEG 400, 0.1M BIS-TRIS PH 6.5

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