2Y8K
Structure of CtGH5-CBM6, an arabinoxylan-specific xylanase.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | ADSC CCD |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 69.120, 75.550, 105.970 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 35.580 - 1.470 |
R-factor | 0.14685 |
Rwork | 0.146 |
R-free | 0.16627 |
Structure solution method | SAD |
Starting model (for MR) | NONE |
RMSD bond length | 0.014 |
RMSD bond angle | 1.448 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | SHELXCDE |
Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 36.740 | 1.550 |
High resolution limit [Å] | 1.470 | 1.470 |
Rmerge | 0.080 | 0.640 |
Number of reflections | 94925 | |
<I/σ(I)> | 13.9 | 2.8 |
Completeness [%] | 99.9 | 99.9 |
Redundancy | 7 | 6.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 20% PEG 3000, 150 MM SODIUM CITRATE, PH 5.5 | |||
1 | 20% PEG 3000, 150 MM SODIUM CITRATE, PH 5.5 |