2Y7M
Structure of N-terminal domain of Candida albicans als9-2 (Pt derivative)
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06DA |
| Synchrotron site | SLS |
| Beamline | X06DA |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2009-10-11 |
| Detector | MARRESEARCH |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 34.723, 68.717, 120.017 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 19.880 - 1.980 |
| R-factor | 0.20852 |
| Rwork | 0.206 |
| R-free | 0.25993 |
| Structure solution method | SIRAS |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.023 |
| RMSD bond angle | 1.896 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | SHARP |
| Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 68.900 | 1.930 |
| High resolution limit [Å] | 1.830 | 1.830 |
| Rmerge | 0.080 | 0.450 |
| Number of reflections | 26698 | |
| <I/σ(I)> | 24.9 | 5.6 |
| Completeness [%] | 99.7 | 98.2 |
| Redundancy | 13.7 | 12.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
