2Y7A
Crystal structure of unliganded GTB P156L
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RUH3R |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Detector | RIGAKU IMAGE PLATE |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 63.730, 78.290, 143.740 |
Unit cell angles | 90.00, 88.96, 90.00 |
Refinement procedure
Resolution | 143.760 - 2.060 |
R-factor | 0.21716 |
Rwork | 0.216 |
R-free | 0.24453 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1ziz |
RMSD bond length | 0.007 |
RMSD bond angle | 0.984 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 143.760 | 2.160 |
High resolution limit [Å] | 2.060 | 2.060 |
Rmerge | 0.070 | 0.350 |
Number of reflections | 75523 | |
<I/σ(I)> | 12.6 | 2.6 |
Completeness [%] | 93.2 | 77.6 |
Redundancy | 2.5 | 2.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7 | 5 MM MOPS PH 7, 1 MM MNCL2, 1 MM DTT, 0.1 M AMSO4, 10% (W/V) PEG 3350. |