2Y4Y
Structure of a domain from the type IV pilus biogenesis lipoprotein PilP, from Pseudomonas aeruginosa
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I02 |
Synchrotron site | Diamond |
Beamline | I02 |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | ADSC QUANTUM 4 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 103.200, 74.510, 74.180 |
Unit cell angles | 90.00, 125.80, 90.00 |
Refinement procedure
Resolution | 32.220 - 1.700 |
R-factor | 0.181 |
Rwork | 0.178 |
R-free | 0.22400 |
Structure solution method | MAD |
Starting model (for MR) | NONE |
RMSD bond length | 0.029 |
RMSD bond angle | 2.298 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | CRANK |
Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 32.000 | 1.790 |
High resolution limit [Å] | 1.700 | 1.700 |
Rmerge | 0.060 | 0.290 |
Number of reflections | 47367 | |
<I/σ(I)> | 8.9 | 2.6 |
Completeness [%] | 94.7 | 92.6 |
Redundancy | 7.3 | 7.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 8.5 | 0.1M TRIS-HCL PH 8.5, 0.6M ZINC ACETATE |