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2Y3U

Crystal structure of apo collagenase G from Clostridium histolyticum at 2.55 Angstrom resolution

Experimental procedure
Experimental methodMAD
Source typeSYNCHROTRON
Source detailsBESSY BEAMLINE 14.1
Synchrotron siteBESSY
Beamline14.1
Temperature [K]100
Detector technologyCCD
Collection date2010-08-12
DetectorMARMOSAIC 225 mm CCD
Spacegroup nameP 21 21 21
Unit cell lengths56.960, 109.050, 182.460
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution40.000 - 2.550
R-factor0.21043
Rwork0.208
R-free0.25645
Structure solution methodMAD
Starting model (for MR)NONE
RMSD bond length0.011
RMSD bond angle1.152
Data reduction softwareiMOSFLM
Data scaling softwareSCALA
Refinement softwareREFMAC (5.5.0109)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]48.3202.690
High resolution limit [Å]2.5502.550
Rmerge0.1000.700
Number of reflections33182
<I/σ(I)>9.31.8
Completeness [%]88.184.4
Redundancy5.45
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
18.321.5% PEG 3350, 0.225 M TRISODIUM CITRATE PH 8.3.

217705

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