2Y3G
Se-Met form of Cupriavidus metallidurans CH34 CnrXs
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE BM30A |
Synchrotron site | ESRF |
Beamline | BM30A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-12-18 |
Detector | MARRESEARCH |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 31.896, 81.809, 93.336 |
Unit cell angles | 90.00, 90.47, 90.00 |
Refinement procedure
Resolution | 46.666 - 1.910 |
R-factor | 0.1899 |
Rwork | 0.187 |
R-free | 0.23820 |
Structure solution method | SAD |
Starting model (for MR) | NONE |
RMSD bond length | 0.006 |
RMSD bond angle | 0.893 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | SHARP |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.670 | 2.010 |
High resolution limit [Å] | 1.910 | 1.910 |
Rmerge | 0.040 | 0.230 |
Number of reflections | 36868 | |
<I/σ(I)> | 13.9 | 3.3 |
Completeness [%] | 99.0 | 95.9 |
Redundancy | 6.2 | 5.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7.5 | 16% PEG 2000MME, 15% GLYCEROL., pH 7.5 |