2Y1J
CRYSTAL STRUCTURE OF A R-DIASTEREOMER ANALOGUE OF THE SPORE PHOTOPRODUCT IN COMPLEX WITH FRAGMENT DNA POLYMERASE I FROM BACILLUS STEAROTHERMOPHILUS
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | MARRESEARCH |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 88.525, 93.382, 105.773 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 46.840 - 2.150 |
R-factor | 0.20061 |
Rwork | 0.199 |
R-free | 0.24103 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1u45 |
RMSD bond length | 0.016 |
RMSD bond angle | 1.529 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.270 |
High resolution limit [Å] | 2.150 | 2.150 |
Rmerge | 0.090 | 0.450 |
Number of reflections | 47859 | |
<I/σ(I)> | 14.9 | 3.7 |
Completeness [%] | 99.3 | 96 |
Redundancy | 4.8 | 4.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |