2XYR
Crystal structure of the nsp16 nsp10 SARS coronavirus complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-12-21 |
Detector | ADSC CCD |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 67.974, 184.107, 129.206 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 19.930 - 2.500 |
R-factor | 0.2026 |
Rwork | 0.201 |
R-free | 0.23517 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2fyg |
RMSD bond length | 0.011 |
RMSD bond angle | 1.254 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 45.580 | 2.640 |
High resolution limit [Å] | 2.500 | 2.500 |
Rmerge | 0.100 | 0.400 |
Number of reflections | 28921 | |
<I/σ(I)> | 12.5 | 4.3 |
Completeness [%] | 100.0 | 100 |
Redundancy | 7.3 | 7.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 9 | 0.1M CHES, 1.52M MGCL2, pH 9 |