Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | MAX II BEAMLINE I911-5 |
| Synchrotron site | MAX II |
| Beamline | I911-5 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2007-12-08 |
| Detector | MARRESEARCH |
| Spacegroup name | P 43 21 2 |
| Unit cell lengths | 139.660, 139.660, 47.790 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 62.458 - 2.510 |
| R-factor | 0.1959 |
| Rwork | 0.194 |
| R-free | 0.24110 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.157 |
| Data reduction software | MOSFLM |
| Data scaling software | XIA |
| Phasing software | PHASER |
| Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 62.460 | 2.570 |
| High resolution limit [Å] | 2.510 | 2.510 |
| Rmerge | 0.100 | 0.730 |
| Number of reflections | 16752 | |
| <I/σ(I)> | 14.6 | 2.9 |
| Completeness [%] | 99.9 | 100 |
| Redundancy | 7.1 | 7.2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 7.5 | 5MM HEPES PH 7.5, 10% PEG 3350, 0.1M AMMONIUM PHOSPHATE, 10MM TRIMETHYLAMINE HYDROCHLORIDE |
