2XY4
X-RAY STRUCTURE OF ZNUA-WT FROM SALMONELLA ENTERICA
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | BESSY BEAMLINE 14.1 |
Synchrotron site | BESSY |
Beamline | 14.1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-11-13 |
Detector | MARRESEARCH |
Spacegroup name | P 63 |
Unit cell lengths | 143.650, 143.650, 30.811 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 50.000 - 1.710 |
R-factor | 0.21115 |
Rwork | 0.209 |
R-free | 0.24402 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2prs |
RMSD bond length | 0.010 |
RMSD bond angle | 1.226 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | MOLREP |
Refinement software | REFMAC (5.5.0070) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.760 |
High resolution limit [Å] | 1.700 | 1.700 |
Rmerge | 0.070 | 0.400 |
Number of reflections | 40175 | |
<I/σ(I)> | 32.19 | 5.3 |
Completeness [%] | 99.7 | 100 |
Redundancy | 11.6 | 11.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7.5 | AMMONIUM SULPHATE 2.5 M, HEPES 0.1 M PH 7.5, PEG 400 2% . |