Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | MAX II BEAMLINE I911-5 |
Synchrotron site | MAX II |
Beamline | I911-5 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2007-01-24 |
Detector | MARRESEARCH SX-165 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 42.060, 42.060, 202.910 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 24.784 - 1.820 |
R-factor | 0.2051 |
Rwork | 0.203 |
R-free | 0.23950 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 1.052 |
Data reduction software | MOSFLM |
Data scaling software | XIA |
Phasing software | PHASER |
Refinement software | PHENIX |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 28.990 | 1.870 |
High resolution limit [Å] | 1.820 | 1.820 |
Rmerge | 0.040 | 0.500 |
Number of reflections | 19558 | |
<I/σ(I)> | 23.1 | 3 |
Completeness [%] | 99.5 | 95.9 |
Redundancy | 4.6 | 4.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 8.5 | 30 % PEG-4000, 0.2 M SODIUM ACETATE TRIHYDRATE, 0.1 M TRIS HYDROCHLORIDE PH 8.5. |