2XVC
Molecular and structural basis of ESCRT-III recruitment to membranes during archaeal cell division
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I02 |
Synchrotron site | Diamond |
Beamline | I02 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-01-21 |
Detector | ADSC CCD |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 65.240, 65.240, 60.992 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 56.500 - 2.150 |
R-factor | 0.22986 |
Rwork | 0.229 |
R-free | 0.25425 |
Structure solution method | SAD |
Starting model (for MR) | NONE |
RMSD bond length | 0.008 |
RMSD bond angle | 1.010 |
Data reduction software | MOSFLM |
Data scaling software | SCALEPACK |
Phasing software | SHARP |
Refinement software | REFMAC (5.5.0088) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 60.990 | 2.270 |
High resolution limit [Å] | 2.150 | 2.150 |
Rmerge | 0.070 | 0.620 |
Number of reflections | 8461 | |
<I/σ(I)> | 24 | 5.6 |
Completeness [%] | 99.7 | 100 |
Redundancy | 10.7 | 20.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 4 | 15% PEG 4000, 5 MM CDCL2, PH 4 |