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2XSK

E. coli curli protein CsgC - SeCys

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSOLEIL BEAMLINE PROXIMA 1
Synchrotron siteSOLEIL
BeamlinePROXIMA 1
Temperature [K]100
Detector technologyCCD
Collection date2009-07-17
DetectorADSC CCD
Spacegroup nameC 1 2 1
Unit cell lengths79.270, 36.150, 39.510
Unit cell angles90.00, 117.09, 90.00
Refinement procedure
Resolution26.660 - 1.700
R-factor0.23929
Rwork0.237
R-free0.28510
Structure solution methodSAD
Starting model (for MR)NONE
RMSD bond length0.021
RMSD bond angle2.128
Data reduction softwareXDS
Data scaling softwareXDS
Phasing softwareSHELX
Refinement softwareREFMAC (5.5.0109)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]32.2001.800
High resolution limit [Å]1.7001.700
Rmerge0.0400.410
Number of reflections11136
<I/σ(I)>16.82.6
Completeness [%]98.898.3
Redundancy3
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
14.6pH 4.6

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PDB entries from 2024-11-06

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