2XSI
Human serum albumin complexed with dansyl-L-glutamate and myristic acid
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SRS BEAMLINE PX9.6 |
| Synchrotron site | SRS |
| Beamline | PX9.6 |
| Temperature [K] | 298 |
| Detector technology | CCD |
| Collection date | 2002-05-02 |
| Detector | ADSC QUANTUM |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 189.260, 38.950, 95.390 |
| Unit cell angles | 90.00, 105.46, 90.00 |
Refinement procedure
| Resolution | 22.370 - 2.700 |
| R-factor | 0.191 |
| Rwork | 0.191 |
| R-free | 0.25100 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1e7g |
| RMSD bond length | 0.007 |
| RMSD bond angle | 1.200 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Phasing software | CNS |
| Refinement software | CNS (1.1) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 21.400 | 2.870 |
| High resolution limit [Å] | 2.700 | 2.700 |
| Rmerge | 0.060 | 0.320 |
| Number of reflections | 18820 | |
| <I/σ(I)> | 12.1 | 3.6 |
| Completeness [%] | 98.5 | 99.3 |
| Redundancy | 2.8 | 2.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 7 | SEE PAPER, pH 7 |
