Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Temperature [K] | 287 |
Detector technology | AREA DETECTOR |
Detector | MULTIWIRE |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 59.600, 102.400, 56.100 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 24.634 - 2.052 |
R-factor | 0.1448 |
Rwork | 0.142 |
R-free | 0.19170 |
Structure solution method | MIR |
Starting model (for MR) | NONE |
RMSD bond length | 0.010 |
RMSD bond angle | 0.948 |
Phasing software | MLPHARE |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 24.600 |
High resolution limit [Å] | 2.050 |
Number of reflections | 19617 |
Completeness [%] | 88.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7 | 12% PEG8000, 50 MM MOPS PH7.0 |