2XR1
DIMERIC ARCHAEAL CLEAVAGE AND POLYADENYLATION SPECIFICITY FACTOR WITH N-TERMINAL KH DOMAINS (KH-CPSF) FROM METHANOSARCINA MAZEI
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2010-05-08 |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 77.660, 97.720, 90.720 |
Unit cell angles | 90.00, 98.26, 90.00 |
Refinement procedure
Resolution | 38.430 - 2.590 |
R-factor | 0.21203 |
Rwork | 0.209 |
R-free | 0.26678 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2i7v |
RMSD bond length | 0.015 |
RMSD bond angle | 1.483 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | MOLREP |
Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 38.600 | 2.750 |
High resolution limit [Å] | 2.600 | 2.600 |
Rmerge | 0.070 | 0.570 |
Number of reflections | 41154 | |
<I/σ(I)> | 13.59 | 2.09 |
Completeness [%] | 98.9 | 95.8 |
Redundancy | 3.43 | 3.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 8 | 20%(W/V) PEG3350, 200MM SODIUM NITRATE, pH 8 |