2XPO
Crystal structure of a Spt6-Iws1(Spn1) complex from Encephalitozoon cuniculi, Form II
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-1 |
Synchrotron site | ESRF |
Beamline | ID14-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2008-12-11 |
Detector | ADSC CCD |
Spacegroup name | P 65 |
Unit cell lengths | 112.578, 112.578, 51.481 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 97.500 - 2.100 |
R-factor | 0.19031 |
Rwork | 0.188 |
R-free | 0.23862 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2xpl |
RMSD bond length | 0.019 |
RMSD bond angle | 1.639 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.150 |
High resolution limit [Å] | 2.100 | 2.100 |
Rmerge | 0.080 | 0.290 |
Number of reflections | 21935 | |
<I/σ(I)> | 33.6 | 10.47 |
Completeness [%] | 99.9 | 100 |
Redundancy | 10.7 | 10.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 5 | 0.1 M SODIUM ACETATE 18% PEG1500 0.05 M MGCL2 |