2XPI
Crystal structure of APC/C hetero-tetramer Cut9-Hcn1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I02 |
Synchrotron site | Diamond |
Beamline | I02 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-01-26 |
Detector | ADSC CCD |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 54.400, 151.920, 91.870 |
Unit cell angles | 90.00, 90.84, 90.00 |
Refinement procedure
Resolution | 54.394 - 2.600 |
R-factor | 0.1908 |
Rwork | 0.189 |
R-free | 0.24520 |
Structure solution method | SAD |
Starting model (for MR) | NONE |
RMSD bond length | 0.010 |
RMSD bond angle | 1.247 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHENIX |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 78.610 | 2.740 |
High resolution limit [Å] | 2.600 | 2.600 |
Rmerge | 0.120 | 0.680 |
Number of reflections | 45418 | |
<I/σ(I)> | 9.1 | 2.5 |
Completeness [%] | 99.2 | 96.4 |
Redundancy | 5.5 | 4.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7.5 | 100 MM HEPES (PH 7.5), 100 MM SODIUM ACETATE, 12.5% (W/V) PEG 3350 |