2XOM
Atomic resolution structure of TmCBM61 in complex with beta-1,4- galactotriose
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL9-2 |
Synchrotron site | SSRL |
Beamline | BL9-2 |
Temperature [K] | 113 |
Detector technology | CCD |
Detector | MARRESEARCH |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 82.915, 31.920, 67.790 |
Unit cell angles | 90.00, 128.28, 90.00 |
Refinement procedure
Resolution | 17.740 - 0.950 |
R-factor | 0.10458 |
Rwork | 0.104 |
R-free | 0.11970 |
Structure solution method | DIRECT METHODS |
Starting model (for MR) | NONE |
RMSD bond length | 0.021 |
RMSD bond angle | 2.025 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | ACORN |
Refinement software | REFMAC (5.5.0072) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 1.000 |
High resolution limit [Å] | 0.950 | 0.950 |
Rmerge | 0.040 | 0.210 |
Number of reflections | 77217 | |
<I/σ(I)> | 26.6 | 5.4 |
Completeness [%] | 92.5 | 68.4 |
Redundancy | 6.4 | 3.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |