2XMU
Copper chaperone Atx1 from Synechocystis PCC6803 (Cu2 form)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID29 |
Synchrotron site | ESRF |
Beamline | ID29 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2008-07-10 |
Detector | ADSC CCD |
Spacegroup name | P 1 |
Unit cell lengths | 29.243, 29.388, 38.702 |
Unit cell angles | 91.69, 101.26, 118.62 |
Refinement procedure
Resolution | 37.580 - 1.750 |
R-factor | 0.26915 |
Rwork | 0.267 |
R-free | 0.31157 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2xmj |
RMSD bond length | 0.014 |
RMSD bond angle | 1.536 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.5.0035) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 25.570 | 1.840 |
High resolution limit [Å] | 1.750 | 1.750 |
Rmerge | 0.060 | 0.300 |
Number of reflections | 10938 | |
<I/σ(I)> | 22 | 9.7 |
Completeness [%] | 98.4 | 97.6 |
Redundancy | 6.8 | 6.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7.5 | 28 % (W/V) PEG 8000, 200 MM SODIUM ACETATE, 100 HEPES PH 7.5 | ||
1 | 7.5 | 28 % (W/V) PEG 8000, 200 MM SODIUM ACETATE, 100 HEPES PH 7.5 |