2XMT
Copper chaperone Atx1 from Synechocystis PCC6803 (Cu1 form)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID29 |
Synchrotron site | ESRF |
Beamline | ID29 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2008-07-10 |
Detector | ADSC CCD |
Spacegroup name | P 1 |
Unit cell lengths | 29.090, 29.660, 38.430 |
Unit cell angles | 100.89, 92.58, 117.91 |
Refinement procedure
Resolution | 25.000 - 1.500 |
R-factor | 0.16256 |
Rwork | 0.160 |
R-free | 0.20279 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2xmj |
RMSD bond length | 0.016 |
RMSD bond angle | 1.494 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.5.0035) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 25.000 | 1.580 |
High resolution limit [Å] | 1.500 | 1.500 |
Rmerge | 0.050 | 0.370 |
Number of reflections | 15929 | |
<I/σ(I)> | 18.2 | 3.9 |
Completeness [%] | 90.3 | 88.1 |
Redundancy | 3.8 | 3.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7.5 | 28%(W/V) PEG 8000, 200MM SODIUM ACETATE, 100MM SODIUM CACODYLATE PH 7.5 |