2XMO
The crystal structure of Lmo2642
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PAL/PLS BEAMLINE 4A |
Synchrotron site | PAL/PLS |
Beamline | 4A |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | ADSC CCD |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 62.963, 103.267, 73.765 |
Unit cell angles | 90.00, 102.80, 90.00 |
Refinement procedure
Resolution | 30.000 - 1.700 |
R-factor | 0.2118 |
Rwork | 0.212 |
R-free | 0.24250 |
Structure solution method | SAD |
Starting model (for MR) | NONE |
RMSD bond length | 0.005 |
RMSD bond angle | 1.247 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | SOLVE |
Refinement software | CNS (1.2) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 1.730 |
High resolution limit [Å] | 1.700 | 1.700 |
Rmerge | 0.090 | 0.390 |
Number of reflections | 93909 | |
<I/σ(I)> | 13.8 | 1.5 |
Completeness [%] | 93.1 | 63.2 |
Redundancy | 5.4 | 3.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7.2 | 20% PEG3350, 0.4M SODIUM FORMATE, pH 7.2 |