2XMJ
Visualising the Metal-binding Versatility of Copper Trafficking Sites: Atx1 side-to-side (aerobic)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-2 |
Synchrotron site | ESRF |
Beamline | ID14-2 |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | ADSC CCD |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 63.460, 41.654, 55.832 |
Unit cell angles | 90.00, 107.70, 90.00 |
Refinement procedure
Resolution | 10.000 - 1.080 |
R-free | 0.14880 |
Structure solution method | AB INITIO PHASING |
Starting model (for MR) | NONE |
RMSD bond length | 0.014 |
RMSD bond angle | 0.032 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | ACORN |
Refinement software | SHELX |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 13.810 | 1.140 |
High resolution limit [Å] | 1.080 | 1.080 |
Rmerge | 0.060 | 0.230 |
Number of reflections | 56359 | |
<I/σ(I)> | 17.9 | 4.4 |
Completeness [%] | 95.9 | 92.8 |
Redundancy | 6.4 | 6.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6.5 | 25 % (W/V) PEG 8000, 200 MM SODIUM ACETATE, 100 MM SODIUM CACODYLATE PH 6.5 |