2XLO
Cytochrome c prime from Alcaligenes xylosoxidans: Ferrous R124E variant with bound NO
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | CLSI BEAMLINE 08ID-1 |
Synchrotron site | CLSI |
Beamline | 08ID-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | MARRESEARCH |
Spacegroup name | P 65 2 2 |
Unit cell lengths | 54.110, 54.110, 181.336 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 46.880 - 1.240 |
R-factor | 0.17558 |
Rwork | 0.174 |
R-free | 0.19960 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.019 |
RMSD bond angle | 1.985 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | MOLREP |
Refinement software | REFMAC (5.5.0066) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 28.700 | 1.180 |
High resolution limit [Å] | 1.140 | 1.140 |
Rmerge | 0.040 | 0.330 |
Number of reflections | 58038 | |
<I/σ(I)> | 35 | 3 |
Completeness [%] | 98.7 | 88.6 |
Redundancy | 8.7 | 4.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7.5 | AMMONIUM SULPHATE, HEPES PH 7.5 |