2XLD
Cytochrome c prime from Alcaligenes xylosoxidans: Ferrous R124Q variant
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | P 65 2 2 |
Unit cell lengths | 53.230, 53.230, 181.510 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 44.680 - 1.400 |
R-factor | 0.18813 |
Rwork | 0.187 |
R-free | 0.21966 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.021 |
RMSD bond angle | 2.107 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | MOLREP |
Refinement software | REFMAC (5.5.0106) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 45.000 | 1.500 |
High resolution limit [Å] | 1.400 | 1.400 |
Rmerge | 0.050 | 0.760 |
Number of reflections | 31045 | |
<I/σ(I)> | 19 | 3 |
Completeness [%] | 95.0 | 84.1 |
Redundancy | 7 | 7.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7.4 | AMMONIUM SULPHATE, HEPES PH 7.5 |