2XJY
Crystal structure of the LMO2:LDB1-LID complex, P21 crystal form
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-2 |
Synchrotron site | ESRF |
Beamline | ID23-2 |
Temperature [K] | 77 |
Detector technology | CCD |
Collection date | 2009-05-15 |
Detector | MARRESEARCH |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 25.140, 54.360, 61.800 |
Unit cell angles | 90.00, 95.45, 90.00 |
Refinement procedure
Resolution | 40.740 - 2.400 |
R-factor | 0.2024 |
Rwork | 0.201 |
R-free | 0.22890 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1rut |
RMSD bond length | 0.008 |
RMSD bond angle | 1.050 |
Data reduction software | xia2 |
Data scaling software | xia2 |
Phasing software | MOLREP |
Refinement software | BUSTER (2.9.2) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.470 |
High resolution limit [Å] | 2.400 | 2.400 |
Rmerge | 0.120 | 0.920 |
Number of reflections | 6395 | |
<I/σ(I)> | 12.3 | 1.2 |
Completeness [%] | 97.8 | 95.8 |
Redundancy | 3.6 | 3.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 4 | 25% PEG 1500 AND 100 MM SPG, BUFFER PH 4.0 |