2XIT
Crystal structure of monomeric MipZ
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2008-05-08 |
Detector | ADSC CCD |
Spacegroup name | H 3 2 |
Unit cell lengths | 124.670, 124.670, 239.050 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 49.270 - 1.800 |
R-factor | 0.18524 |
Rwork | 0.184 |
R-free | 0.23040 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.011 |
RMSD bond angle | 1.294 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | REFMAC (5.5.0102) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.200 | 1.830 |
High resolution limit [Å] | 1.800 | 1.800 |
Rmerge | 0.060 | 0.380 |
Number of reflections | 66140 | |
<I/σ(I)> | 21 | 4.9 |
Completeness [%] | 99.9 | 100 |
Redundancy | 6 | 5.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7.5 | pH 7.5 |