2XHR
Structure of HSP90 with small molecule inhibitor bound
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Temperature [K] | 100 |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 65.652, 89.559, 99.181 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 36.200 - 2.200 |
R-factor | 0.2532 |
Rwork | 0.251 |
R-free | 0.30360 |
Structure solution method | OTHER |
Starting model (for MR) | NONE |
Refinement software | BUSTER-TNT (2.5.1) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 36.190 |
High resolution limit [Å] | 2.200 |
Rmerge | 0.100 |
Number of reflections | 15199 |
Completeness [%] | 99.2 |
Redundancy | 2.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |