Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | C 2 2 2 |
Unit cell lengths | 130.609, 222.551, 86.201 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 14.990 - 2.200 |
R-factor | 0.18946 |
Rwork | 0.188 |
R-free | 0.23925 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1OJB |
RMSD bond length | 0.010 |
RMSD bond angle | 1.256 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | AMoRE |
Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.000 | 2.320 |
High resolution limit [Å] | 2.200 | 2.200 |
Rmerge | 0.130 | 0.470 |
Number of reflections | 64040 | |
<I/σ(I)> | 4.9 | 1.7 |
Completeness [%] | 99.9 | 99.9 |
Redundancy | 3.7 | 3.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6.5 | pH 6.5 |