2XEU
Ring domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-4 |
Synchrotron site | ESRF |
Beamline | ID14-4 |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | ADSC QUANTUM 315r |
Spacegroup name | P 41 3 2 |
Unit cell lengths | 72.616, 72.616, 72.616 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 18.150 - 1.500 |
R-factor | 0.16972 |
Rwork | 0.168 |
R-free | 0.19727 |
Structure solution method | SAD |
Starting model (for MR) | NONE |
RMSD bond length | 0.009 |
RMSD bond angle | 1.439 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | SHELX |
Refinement software | REFMAC (5.6.0073) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 18.000 | 1.550 |
High resolution limit [Å] | 1.500 | 1.500 |
Rmerge | 0.060 | 0.430 |
Number of reflections | 10402 | |
<I/σ(I)> | 18 | 2.9 |
Completeness [%] | 99.8 | 100 |
Redundancy | 9 | 7.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |