2XEQ
Human PatL1 C-terminal domain
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X10SA |
| Synchrotron site | SLS |
| Beamline | X10SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2008-12-08 |
| Detector | DECTRIS PILATUS 6M |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 102.160, 108.570, 108.820 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 43.919 - 3.100 |
| R-factor | 0.2491 |
| Rwork | 0.247 |
| R-free | 0.28160 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 2xes |
| RMSD bond length | 0.005 |
| RMSD bond angle | 0.680 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | PHASER |
| Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 43.900 | 3.180 |
| High resolution limit [Å] | 3.100 | 3.100 |
| Number of reflections | 22432 | |
| <I/σ(I)> | 9.1 | 1.9 |
| Completeness [%] | 99.4 | 99.9 |
| Redundancy | 4.7 | 4.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 7.8 | 0.1 M BIS-TRIS-PROPANE, PH 7.8, 10% PEG3350, 0.2 M NA3-CITRATE |
