2XEH
Structural Determinants for Improved Thermal Stability of Designed Ankyrin Repeat Proteins With a Redesigned C-capping Module.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | P 61 |
Unit cell lengths | 128.905, 128.905, 50.696 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 42.194 - 1.810 |
R-factor | 0.2172 |
Rwork | 0.217 |
R-free | 0.24970 |
Structure solution method | OTHER |
Starting model (for MR) | NONE |
RMSD bond length | 0.004 |
RMSD bond angle | 0.803 |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 1.800 |
Rmerge | 0.070 |
Number of reflections | 44196 |
Completeness [%] | 99.4 |
Redundancy | 6.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |