2XEE
Structural Determinants for Improved Thermal Stability of Designed Ankyrin Repeat Proteins With a Redesigned C-capping Module.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 62.050, 62.050, 270.180 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 49.931 - 2.100 |
R-factor | 0.1788 |
Rwork | 0.175 |
R-free | 0.24000 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2qyj |
RMSD bond length | 0.002 |
RMSD bond angle | 0.460 |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 2.100 |
Rmerge | 0.090 |
Number of reflections | 35848 |
Completeness [%] | 98.2 |
Redundancy | 5.63 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |