2XDK
Structure of HSP90 with small molecule inhibitor bound
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Temperature [K] | 100 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 53.591, 44.211, 54.298 |
| Unit cell angles | 90.00, 115.89, 90.00 |
Refinement procedure
| Resolution | 32.780 - 1.970 |
| R-factor | 0.1747 |
| Rwork | 0.171 |
| R-free | 0.24040 |
| Structure solution method | OTHER |
| Starting model (for MR) | NONE |
| Refinement software | BUSTER-TNT (2.5.1) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 32.800 |
| High resolution limit [Å] | 1.970 |
| Rmerge | 0.070 |
| Number of reflections | 15655 |
| <I/σ(I)> | 4.4 |
| Completeness [%] | 98.0 |
| Redundancy | 2.1 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
