2XD3
The crystal structure of MalX from Streptococcus pneumoniae in complex with maltopentaose.
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Temperature [K] | 113 |
| Spacegroup name | P 21 21 2 |
| Unit cell lengths | 68.370, 127.880, 51.990 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 20.000 - 2.000 |
| R-factor | 0.2089 |
| Rwork | 0.207 |
| R-free | 0.25063 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 2gha |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.267 |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 20.000 | 2.050 |
| High resolution limit [Å] | 2.000 | 2.000 |
| Rmerge | 0.060 | 0.310 |
| Number of reflections | 29101 | |
| <I/σ(I)> | 17.3 | 3.5 |
| Completeness [%] | 92.7 | 94.1 |
| Redundancy | 4.3 | 4.1 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
