2XD2
The crystal structure of MalX from Streptococcus pneumoniae
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Temperature [K] | 113 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 181.305, 56.940, 113.690 |
| Unit cell angles | 90.00, 128.83, 90.00 |
Refinement procedure
| Resolution | 20.000 - 2.900 |
| R-factor | 0.21885 |
| Rwork | 0.216 |
| R-free | 0.27392 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.007 |
| RMSD bond angle | 1.062 |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.5.0072) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 20.000 | 2.970 |
| High resolution limit [Å] | 2.900 | 2.900 |
| Rmerge | 0.110 | 0.420 |
| Number of reflections | 85794 | |
| <I/σ(I)> | 10.9 | 3.4 |
| Completeness [%] | 96.4 | 95.4 |
| Redundancy | 4.4 | 4.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
