2XCY
Crystal structure of Aspergillus fumigatus sialidase
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-02-23 |
Detector | RIGAKU CCD |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 75.890, 58.190, 94.700 |
Unit cell angles | 90.00, 100.01, 90.00 |
Refinement procedure
Resolution | 12.400 - 1.840 |
R-factor | 0.15528 |
Rwork | 0.153 |
R-free | 0.19406 |
Structure solution method | SAD |
Starting model (for MR) | NONE |
RMSD bond length | 0.009 |
RMSD bond angle | 1.134 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | SHELX |
Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 12.400 | 1.940 |
High resolution limit [Å] | 1.840 | 1.840 |
Rmerge | 0.060 | 0.200 |
Number of reflections | 59980 | |
<I/σ(I)> | 15.6 | 5.2 |
Completeness [%] | 84.2 | 64.8 |
Redundancy | 3.1 | 3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |