2X9C

Crystal structure of a soluble PrgI mutant from Salmonella Typhimurium

Refinement Statistics

Experimental method:X-RAY DIFFRACTION (2.45 Å)

Cell axes64.53064.530104.290
Cell angles90.0090.00120.00
SpacegroupP 31 1 2
Resolution limits38.13 - 2.45
the highest resolution shell value2.600 - 2.450
R-factor0.225
R-work0.22500
the highest resolution shell value0.439
R-free0.23900
the highest resolution shell value0.542
RMSD bond length0.008
RMSD bond angle1.100

Data Collection Statistics

Resolution limits50.00 - 2.25
the highest resolution shell value -
Number of reflections11435
Rmerge_l_obs0.110
the highest resolution shell value0.920
Completeness94.9
Redundancy7.5
the highest resolution shell value7.6
I/sigma(I)-3

Crystallization Conditions

crystal IDmethodpHpH rangetemperatureunit
1VAPOR DIFFUSION, HANGING DROP

Crystallization Reagents

IDcrystal IDsolution IDreagent nameconcentrationdetails
Crystallization Reagents in Literatures*
IDcrystal IDsolutionreagent nameconcentration (unit)details
Annotated Information is extracted from Literature Info*