2X96
Crystal structure of AnCE-RXPA380 complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I02 |
Synchrotron site | Diamond |
Beamline | I02 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-08-07 |
Detector | ADSC CCD |
Spacegroup name | H 3 |
Unit cell lengths | 173.068, 173.068, 101.584 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 32.710 - 1.850 |
R-factor | 0.19503 |
Rwork | 0.194 |
R-free | 0.21478 |
Structure solution method | MOLECULAR REPLACEMENT |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | REFMAC (5.5.0072) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.920 |
High resolution limit [Å] | 1.850 | 1.850 |
Rmerge | 0.090 | 0.240 |
Number of reflections | 96897 | |
<I/σ(I)> | 10.1 | 3.7 |
Completeness [%] | 91.0 | 66.6 |
Redundancy | 2.8 | 2.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7.5 | pH 7.5 |