2X87
Crystal Structure of the reconstituted CotA
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 110 |
Detector technology | CCD |
Detector | ADSC CCD |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 101.300, 101.300, 136.092 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 40.290 - 2.000 |
R-factor | 0.1724 |
Rwork | 0.171 |
R-free | 0.19812 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1w6l |
RMSD bond length | 0.009 |
RMSD bond angle | 1.124 |
Phasing software | MOLREP |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.290 | 2.110 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.070 | 0.380 |
Number of reflections | 54422 | |
Completeness [%] | 99.0 | 99.7 |
Redundancy | 4.9 | 4.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |