2X7Q
The conserved Candida albicans CA3427 gene product defines a new family of proteins exhibiting the generic periplasmic binding protein structural fold
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID29 |
Synchrotron site | ESRF |
Beamline | ID29 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2004-12-03 |
Detector | ADSC CCD |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 41.411, 65.724, 128.203 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 23.887 - 2.000 |
R-factor | 0.2186 |
Rwork | 0.218 |
R-free | 0.23640 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2x7p |
RMSD bond length | 0.002 |
RMSD bond angle | 0.478 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | AMoRE |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 128.200 | 2.110 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.100 | 0.260 |
Number of reflections | 17895 | |
<I/σ(I)> | 6.5 | 2.7 |
Completeness [%] | 76.7 | 72.6 |
Redundancy | 8 | 6.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |