2X64
GLUTATHIONE-S-TRANSFERASE FROM XYLELLA FASTIDIOSA
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2006-11-15 |
Detector | MAR scanner 345 mm plate |
Spacegroup name | P 1 |
Unit cell lengths | 47.670, 87.890, 90.780 |
Unit cell angles | 116.53, 99.33, 94.49 |
Refinement procedure
Resolution | 33.670 - 2.300 |
R-factor | 0.1694 |
Rwork | 0.167 |
R-free | 0.21910 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.010 |
RMSD bond angle | 1.060 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | BUSTER (2.8.0) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.350 | 2.420 |
High resolution limit [Å] | 2.300 | 2.300 |
Rmerge | 0.090 | 0.420 |
Number of reflections | 53809 | |
<I/σ(I)> | 7.9 | 1.9 |
Completeness [%] | 94.5 | 92.1 |
Redundancy | 2.1 | 2.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |