2X4I
ORF 114a from Sulfolobus islandicus rudivirus 1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-2 |
Synchrotron site | ESRF |
Beamline | ID14-2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2006-05-13 |
Detector | ADSC QUANTUM 4 |
Spacegroup name | P 43 |
Unit cell lengths | 48.790, 48.790, 195.270 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 27.080 - 2.200 |
R-factor | 0.24319 |
Rwork | 0.241 |
R-free | 0.27736 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2BLK |
RMSD bond length | 0.008 |
RMSD bond angle | 0.986 |
Data reduction software | MOSFLM |
Data scaling software | SCALEPACK |
Phasing software | MOLREP |
Refinement software | REFMAC (5.5.0102) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 27.080 | 2.260 |
High resolution limit [Å] | 2.200 | 2.200 |
Rmerge | 0.060 | 0.660 |
Number of reflections | 16793 | |
<I/σ(I)> | 11.6 | 2.1 |
Completeness [%] | 76.8 | 32.4 |
Redundancy | 3.2 | 3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7.5 | 31% PEG1500, 0.1M HEPES, PH 7.5 |