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2X4I

ORF 114a from Sulfolobus islandicus rudivirus 1

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsESRF BEAMLINE ID14-2
Synchrotron siteESRF
BeamlineID14-2
Temperature [K]100
Detector technologyCCD
Collection date2006-05-13
DetectorADSC QUANTUM 4
Spacegroup nameP 43
Unit cell lengths48.790, 48.790, 195.270
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution27.080 - 2.200
R-factor0.24319
Rwork0.241
R-free0.27736
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)2BLK
RMSD bond length0.008
RMSD bond angle0.986
Data reduction softwareMOSFLM
Data scaling softwareSCALEPACK
Phasing softwareMOLREP
Refinement softwareREFMAC (5.5.0102)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]27.0802.260
High resolution limit [Å]2.2002.200
Rmerge0.0600.660
Number of reflections16793
<I/σ(I)>11.62.1
Completeness [%]76.832.4
Redundancy3.23
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
17.531% PEG1500, 0.1M HEPES, PH 7.5

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