2X48
ORF 55 from Sulfolobus islandicus rudivirus 1
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID14-4 |
| Synchrotron site | ESRF |
| Beamline | ID14-4 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2007-09-01 |
| Detector | ADSC CCD |
| Spacegroup name | I 2 3 |
| Unit cell lengths | 119.110, 119.110, 119.110 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 84.220 - 2.600 |
| R-factor | 0.22528 |
| Rwork | 0.223 |
| R-free | 0.26657 |
| Structure solution method | OTHER |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.009 |
| RMSD bond angle | 0.997 |
| Data reduction software | XDS |
| Data scaling software | SCALA |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 84.220 | 2.670 |
| High resolution limit [Å] | 2.600 | 2.600 |
| Rmerge | 0.050 | 0.490 |
| Number of reflections | 8384 | |
| <I/σ(I)> | 36 | 7 |
| Completeness [%] | 99.8 | 100 |
| Redundancy | 15.6 | 13.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 8 | PH 8 |
