2X32
Structure of a polyisoprenoid binding domain from Saccharophagus degradans implicated in plant cell wall breakdown
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-2 |
Synchrotron site | ESRF |
Beamline | ID14-2 |
Temperature [K] | 120 |
Detector technology | CCD |
Collection date | 2008-10-05 |
Detector | ADSC QUANTUM 4r |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 63.378, 64.360, 84.732 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 51.230 - 1.550 |
R-factor | 0.16028 |
Rwork | 0.159 |
R-free | 0.19418 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2x34 |
RMSD bond length | 0.019 |
RMSD bond angle | 1.872 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | AMoRE |
Refinement software | REFMAC (5.5.0102) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 35.000 | 1.630 |
High resolution limit [Å] | 1.550 | 1.550 |
Rmerge | 0.060 | 0.480 |
Number of reflections | 51047 | |
<I/σ(I)> | 17.1 | 3.3 |
Completeness [%] | 100.0 | 100 |
Redundancy | 5.9 | 6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 5.5 | pH 5.5 |