2X2V
Structural basis of a novel proton-coordination type in an F1Fo-ATP synthase rotor ring
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2009-04-02 |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 74.180, 97.340, 121.240 |
Unit cell angles | 90.00, 104.73, 90.00 |
Refinement procedure
Resolution | 44.951 - 2.500 |
R-factor | 0.1899 |
Rwork | 0.188 |
R-free | 0.23450 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2wie |
RMSD bond length | 0.007 |
RMSD bond angle | 0.932 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 44.951 | 2.600 |
High resolution limit [Å] | 2.500 | 2.500 |
Rmerge | 0.100 | 0.980 |
Number of reflections | 57111 | |
<I/σ(I)> | 11.7 | 1.62 |
Completeness [%] | 98.8 | 92.8 |
Redundancy | 3.6 | 3.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 4.3 | pH 4.3 |