2X2D
acetyl-CypA:HIV-1 N-term capsid domain complex
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID29 |
| Synchrotron site | ESRF |
| Beamline | ID29 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2009-02-15 |
| Detector | ADSC CCD |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 38.542, 109.995, 67.567 |
| Unit cell angles | 90.00, 101.11, 90.00 |
Refinement procedure
| Resolution | 66.300 - 1.950 |
| R-factor | 0.19974 |
| Rwork | 0.197 |
| R-free | 0.25695 |
| Structure solution method | OTHER |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.021 |
| RMSD bond angle | 1.777 |
| Refinement software | REFMAC (5.5.0100) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 42.300 |
| High resolution limit [Å] | 1.900 |
| Rmerge | 0.160 |
| Number of reflections | 40235 |
| Completeness [%] | 98.2 |
| Redundancy | 3.2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
