2X1P
Gelsolin Nanobody
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | ADSC CCD |
Spacegroup name | P 1 2 1 |
Unit cell lengths | 55.948, 59.342, 81.651 |
Unit cell angles | 90.00, 90.01, 90.00 |
Refinement procedure
Resolution | 19.510 - 1.100 |
R-factor | 0.204 |
Rwork | 0.203 |
R-free | 0.22000 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1hcv |
RMSD bond length | 0.006 |
RMSD bond angle | 1.119 |
Data reduction software | HKL |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 19.750 | 1.140 |
High resolution limit [Å] | 1.100 | 1.100 |
Rmerge | 0.060 | 0.190 |
Number of reflections | 204183 | |
<I/σ(I)> | 23.6 | 3.08 |
Completeness [%] | 99.5 | 99.8 |
Redundancy | 7.2 | 3.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 30% PEG 1000, 100 MM PHOSPHATE/ CITRATE PH 4.4, 100 MM LISO4 |